WebMay 8, 2008 · The invention relates to a preparation method of herbicide bispyribac-sodium, which belongs to the technology field of chemistry industry. The preparation method includes using 2-chloro-4, 6-dimethoxypyrimidine as raw material and 2,6-dihydroxy benzoic acid to directly react in solvent in the presence of sodium alkyl sulfinate as catalyst and ... WebThe invention discloses a crystallization preparation method of cloxacillin sodium. The method is as follows: stirring added 0.03g/mL-0.2g/mL sodium isooctoate-alcohol solution in 0.1-0.2g/mL cloxacillin acid solution at the temperature of 5-25 DEG C, reacting and crystallizing, wherein the pH value of the final point of the reaction process is 5.5-7.5; then …
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